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Field and Laboratory Quality Assurance

Dates

Publication Date
Start Date
2014-04
End Date
2014-09

Citation

Elliott, S.M., Lee, K.E., Brigham, M.E., Langer, S.K., McCool, M.M., Menheer, M.A., Furlong, E.T., Foreman, W.T., Jorgenson, Z.G., Choy, S.J., Moore, J.N., Banda, J.A., Gefell, D.J., and Schoenfuss, H.L., 2016, Chemicals of Emerging Concern in Water and Bottom Sediment in the Great Lakes Basin, 2014 - Analytical Methods, Collection Methods, Quality-Assurance Analyses, and Data: U.S. Geological Survey data release, http://dx.doi.org/10.5066/F7TH8JS6.

Summary

Several quality-control measures were implemented in the field and at the Environmental Sampling Technologies Laboratory and the U.S. Geological Survey National Water Quality Laboratory to evaluate the integrity of the data being generated. Sample replicates and blank samples were collected in the field. Surrogate standards, isotope dilution standards, matrix spikes, reagent blank-water spikes, reagent blank-sand samples, polar organic chemical integrative sampler (POCIS) method blank samples, and POCIS method spikes were prepared in the laboratory. Quality-control measures used in 2014 were similar to those used in previous years of the study. Detailed descriptions and how the quality-control data are used can be found in Lee and [...]

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Attached Files

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2014WaterSedLabBlankDetections.xlsx
“Laboratory Blank Detections in Water and Sediment”
17.38 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014POCISLaboratoryBlankDetections.xlsx
“Laboratory Blank Detections in POCIS”
9.73 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014LaboratoryReagentSpikes.xlsx
“Laboratory Reagent Spike Recoveries”
31.03 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014SurrogateRecoveries.xlsx
“Laboratory Surrogate Recoveries”
17.37 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014POCISMethodSpikeRecovery.xlsx
“POSIC Laboratory Spike Recoveries”
32.47 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014ReplicateSamples.xlsx
“Replicate Sample Statistics”
1.91 MB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014SedimentMatrixSpikeRecovery.xlsx
“Sediment Matrix Spike Recoveries”
21.96 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet
2014WaterMatrixSpikeRecovery.xlsx
“Water Matrix Spike Recoveries”
28.05 KB application/vnd.openxmlformats-officedocument.spreadsheetml.sheet

Purpose

The U.S. Fish and Wildlife Service initiated the study through the Great Lakes Restoration Initiative as an early warning program to detect and identify emerging contaminants and to evaluate the effects of these contaminants on fish and wildlife.

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