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Neonicotinoids have become the most widely used insecticides in world with rapid growth in applications as seed coatings. Nontarget organisms are exposed to concentrated levels of pesticidal active ingredients through ingestion of treated seeds. To better understand pesticide fate, analytical methods are necessary to rapidly screen and accurately quantitate contaminants in environmental and biological matrices. Liquid chromatography-tandem mass spectrometry (LC-MS/MS) is commonly employed for neonicotinoid analyses but requires expensive analytical instrumentation and potentially laborious sample preparation. Enzyme-linked immunosorbent assays (ELISAs) are efficient and sensitive alternative methods for neonicotinoid...
Categories: Data;
Tags: Coturnix japonica,
Environmental Health,
USGS Science Data Catalog (SDC),
United States,
environment,
During November 2018, the Camp Fire burned more than 150,000 acres in Butte County, California. The fire was the deadliest and most destructive in California history, destroying more than 18,000 structures and causing at least 85 fatalities. The U.S. Geological Survey sampled surface water in areas affected by the Camp Fire, plus an unburned control site, during two post-fire sampling events, January 21-23, 2019 and February 28 - March 1, 2019. During each of those two sampling events, surface-water samples were collected at 8 stream locations. These 16 water samples were filtered using filters with multiple pore sizes (1.2 µm, 0.8 µm, 0.45 µm, and 0.22 µm) to evaluate colloid transport of trace elements. The filtrates...
Categories: Data;
Tags: Butte County,
California,
Environmental Health,
Geochemistry,
Land Use Change,
This dataset contains the results from 80 visual encounter surveys at two wetlands in Palmetto Island State Park, Vermillion Parish, Louisiana from August 2015 to April 2019. These surveys mainly targeted snakes but small turtles and anoles were also opportunistically captured. Captured animals were swabbed to determine the prevalence of Ophidiomyces ophiodiicola, the causative agent of Snake Fungal Disease. Physical measurements were taken on all captured individuals. This dataset also includes environmental data such as temperature, water level, and humidity at the study site.
Nitrapyrin is a nitrification inhibitor that is co-applied with N-fertilizer in agroecosystems. Over the course of one year (March 2016 to June 2017), 192 water samples from seven streams across Iowa and Illinois were analyzed for nitrapyrin, its degradate 6-chloropicolinic acid (6-CPA), and three widely used herbicides acetochlor, atrazine, and metolachlor. Additional environmental samples were collected and analyzed in spring 2017: 63 water samples from eight subsurface drains, and 33 soil samples from a field in Iowa that received direct application of nitrapyrin (only for nitrapyrin and herbicides). Nitrapyrin was detected in all seven streams (56% detection) with concentrations ranging from 4 to 1,200 ng/L;...
This dataset describes the quantity and morphology of floating microplastics in 29 Great Lakes tributaries in 6 states. Samples were collected in spring 2014 – spring 2015. Each tributary was sampled three to four times, capturing low-flow and runoff-event conditions. Sampling and analysis methods are described in the .xml metadata file. These data are interpreted in a journal article: Baldwin, A.K., Corsi, S.R., and Mason, S.A., 2016, Plastic debris in 29 Great Lakes tributaries: Relations to watershed attributes and hydrology: Environmental Science and Technology, v. 50, no. 19, p. 10377–10385, doi:10.1021/acs.est.6b02917.
This data release contains analytical results of organohalogenated compounds and mercury in lamprey and sediment that were collected from rivers in Oregon and along the Pacific northwest coast from 2017 to 2021. In 2017, 20 lamprey were collected off the Washington and Oregon coasts by the National Oceanic and Atmospheric Administration. These ocean-caught juvenile lamprey were parasitizing targeted fish and were bycatch. In 2019, larval lamprey were collected by the Confederated Tribes of Warm Springs of Oregon from 8 sites on the Warm Springs Reservation. Larval lamprey were collected by electroshocking depositional sediment areas. Collocated depositional sediment samples also were collected along with the larval...
Categories: Data;
Tags: Aquatic Biology,
Environmental Health,
Oregon,
USGS Science Data Catalog (SDC),
United States,
This dataset contains data from an ongoing trapping effort beginning in 2019 targeting alligator snapping turtles (Macrochelys temminckii) in the Atchafalaya Basin of south-central Louisiana.
This dataset compiles all data used in a study on occupancy of secretive marsh birds collected from automated audio recording units in southwest Louisiana. The main data files consist of detection histories for the 11 species across 20 sampling occasions at 33 sites. The sites were randomly selected, and all site level information is provided, including coordinates, marsh type, and habitat designation for our analysis. The sampling information table provides the date of each sample as well as the environmental conditions used as a covariate of detection in our model.
Four dichloroacetamide herbicide safeners (AD-67, benoxacor, dichlormid, and furilazole) and two co-applied herbicides (acetochlor and metolachlor) were measured in water samples from 7 streams across Iowa and Illinois. Iowa water samples were collected from March 2016 to June 2017, and Illinois water samples were collected from September 2016 to June 2017. The compounds studied are applied to corn, and Iowa and Illinois are the two largest corn producing states in the U.S. The seven stream sites are all adjacent to agricultural fields in corn production. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. With the exception of one site, Iowa River at Wapello (USGS...
Categories: Data;
Tags: Corn Belt region,
Environmental Health,
Illinois,
Iowa,
USGS Science Data Catalog (SDC),
Nitrapyrin, a nitrification inhibitor, 6-CPA, a nitrapyrin degradate, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in surface drains from eights sites in Illinois. Water samples were collected from April to June 2017. The compounds studied are applied to corn, Illinois is one of the largest corn producing states in the U.S. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. Water samples were filtered (0.7 micrometers), extracted via solid phase extraction (Oasis® MAX cartridge), and analyzed (nitrapyrin and herbicides by gas chromatography with mass-spectrometry; 6-CPA by liquid chromatography tandem mass-spectrometry).
Categories: Data;
Tags: Corn Belt region,
Illinois,
United States,
contaminant transport,
ecotoxicity,
Nitrapyrin, a nitrification inhibitor, 6-CPA, a nitrapyrin degradate, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in water samples from seven streams across Iowa and Illinois. Iowa water samples were collected from March 2016 to June 2017, and Illinois water samples were collected from September 2016 to June 2017. The compounds studied are applied to corn, and Iowa and Illinois are the two largest corn producing states in the U.S. The seven stream sites are all adjacent to agricultural fields in corn production. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. With the exception of one site, Iowa River at Wapello (USGS Site...
Nitrapyrin, a nitrification inhibitor, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in soil samples from an agricultural field in Iowa. Samples were collected from three locations in the field before and after nitrapyrin application in April-May 2017. Soils were collected using a 5-inch pipe that was hammered into the ground. Soil samples were extracted using pressurized solvent extraction (with dichloromethane), clean-up via solid phase extraction (carbon and alumina sorbents), and analyzed by gas chromatography with mass-spectrometry.
This dataset contains data on trapping methodology, turtle captures, and environmental variables from a trapping effort targeting alligator snapping turtles (Macrochelys temminckii) in south-central Louisiana in 2019.
Japanese quail (Coturnix japonica) were orally dosed with pesticide-treated or control-untreated wheat seeds. Pesticide treated wheat seeds were analytically verified for active ingredients of imidacloprid, metalaxyl, tebuconazole, and fludioxonil. Pesticide and metabolite residues were measured in plasma, liver, brain, kidney, muscle, and excreta of exposed and control birds. Samples were extracted via solid phase extraction, pressurized liquid extraction, or sonication. Clean-up steps included protein precipitation followed by solid phase extraction. All samples were analyzed by liquid chromatography tandem mass spectrometry.
Categories: Data;
Tags: Coturnix japonica,
Environmental Health,
USGS Science Data Catalog (SDC),
United States,
environment,
Lab-reared colonies of Bombus huntii (Hunt bumble bee) were deployed in a commercial cherry orchard in the spring of 2016. A fungicide formulation containing boscalid (25.2%) and pyraclostrobin (12.8%) was applied one time at the recommended label rate. Nectar and pollen were collected daily, beginning two days before spray application and continuing for ten days following. Nectar samples were extracted with acetonitrile and cleaned up using dispersive solid-phase extraction with primary-secondary amine, C18, and magnesium sulfate. Pollen samples were extracted with ethyl acetate. Both types of samples were analyzed by GC-MS/MS for boscalid and pyraclostrobin. Fungicide concentrations in nectar varied spatially...
Categories: Data;
Tags: Bombus,
Ecology,
Environmental Health,
Oregon,
USGS Science Data Catalog (SDC),
Ultra-low volumes of naled are applied by aircraft over rice fields and canals to reduce adult mosquito populations near Sacramento, California. Each summer, the pesticide is applied approximately 7-10 times between July and October. Naled and its major degradate (dichlorvos) were quantified in water, biofilm, and invertebrates following aerial applications. In 2020, samples were collected before the naled application season, after 3 rice field and 5 canal applications, and immediately after an application. In 2021, water and crayfish samples were collected before the naled application season, after 3 applications, and at intervals (1, 3, 5, and 7 days) following an application. A few opportunistic samples (including...
Categories: Data;
Tags: Aquatic Biology,
California,
Ecology,
USGS Science Data Catalog (SDC),
United States,
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