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A method was described for determination of trace levels of silicon by inductively coupled plasma mass spectrometry (ICP-MS) from hydrofluoric (HF) digests of biological samples. The volatility of silicon in HF digests was examined with synthetic solutions as well as soil and mine waste samples. A digestion scheme was optimized to achieve complete dissolution, avoid loss of volatile silicon species and produce sample solutions that can be directly analyzed by ICP-MS. The performance of the method performance was validated by analysis of a number plant and tissue certified reference materials for silicon by ICP-MS. The method was then applied to the determination of silicon from lung biopsy tissues obtained from...
We tested the hypothesis that the monoterpenoid levels in the ingesta from various digestive organs of sage grouse are less than that expected from the big sagebrush leaves ingested. Results supported the hypothesis. Dramatic reductions occurred between the gizzard and duodenum. Monoterpenoid levels in the ceca were nil; thus adverse effects of monoterpenoids on ceca microbes would also be nil. Published in Journal of Chemical Ecology, volume 15, issue 3, on pages 961 - 969, in 1989.
Juvenile sculpin (Cottus extensus) less than 30 mm long exhibit a diel vertical migration in the limnetic zone of Bear Lake (Utah-Idaho). Using mid-water and bottom trawls we found that these fish inhabit the bottom of the lake (5� C) during the day but migrate 30?40 m into the water column at night where they reside in the metalimnion or epilimnion at temperatures near 13?16�C. Larger fish do not migrate into the water column. Stomach analyses demonstrated that the young-of-the-year fish do not migrate into the water column to feed: from July to October their diet is 70?93% benthic ostracods and copepods, and pelagic prey are rarely consumed. Furthermore, gut fullness of the sculpin increases through the daylight...