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The dataset includes specifics on liver tissue and blood plasma anticoagulant rodenticide concentrations measured using high-performance liquid chromatography-tandem mass spectrometry. This data release supersedes Herring, G., and Eagles-Smith, C.A., 2022, Anticoagulant rodenticide concentrations in blood and tissue of California condors and turkey vultures: U.S. Geological Survey data release, https://doi.org/10.5066/P9NHPLHX. Please contact fresc_outreach@usgs.gov for access.
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Archived plasma from fish health monitoring sites within the Chesapeake Bay watershed was analyzed for 13 perfluoroalkyl compounds. Smallmouth bass were collected from two sites in the Potomac River drainage (Antietam Creek, Maryland and South Branch Potomac, West Virginia) and two in the Susquehanna River drainage (West Branch Mahantango Creek, Pennsylvania and Pine Creek, Pennsylvania). Site and date of collection, length, weight and age of each adult smallmouth bass were documented. Four compounds were detected in every plasma sample, while two additonal compounds were only occasionally observed at low concentrations.
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Pesticides are widely applied and can enter the environment, potentially effecting non-target organisms. To better evaluate pesticide exposure using non-lethal techniques, a method was developed for the extraction of pesticides and their degradates from small (100 µL) volume plasma samples. Solid phase extraction was used for lipid removal after plasma samples were protein precipitated. Samples were analyzed with liquid chromatography and gas chromatography with tandem mass spectrometry. Samples were spiked at three different concentrations, low (25 ng/mL), medium (100 ng/mL), and high (250 ng/mL) and recoveries of 70 to 130% were achieved across all spike levels for 179, 180, and 183 of 210 target compounds were...


    map background search result map search result map Morphometric, Age and Concentrations of Perfluoroalkyl Substances in Smallmouth Bass Plasma from Four Sites in the Chesapeake Bay watershed Anticoagulant rodenticide concentrations in blood and tissue of California condors and turkey vultures (ver. 2.0, May 2023) Pesticides in small volume plasma samples Pesticides in small volume plasma samples Morphometric, Age and Concentrations of Perfluoroalkyl Substances in Smallmouth Bass Plasma from Four Sites in the Chesapeake Bay watershed Anticoagulant rodenticide concentrations in blood and tissue of California condors and turkey vultures (ver. 2.0, May 2023)