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This data release contains reflectance measurements for eight samples submitted to the USGS Organic Petrology Laboratory in Reston. Samples include two artificial rock samples made from cement with organic matter added (samples 001-002), a coal and shale sample (samples 003-004, respectively), and hydrous pyrolysis residues for samples 001-004. The hydrous pyrolysis experiments were conducted at 330°C for 72 hours at the United States Geological Survey's (USGS) Denver Federal Center. Samples were mounted into 1-inch circular briquettes in USGS-Reston according to ASTM D2797 for organic petrographic analysis. Cement plugs (samples 001-002, and pyrolysis residues 005-006) were crushed to approximately 1 mm top-size...
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This study presents Raman spectroscopic data paired with scanning electron microscopy (SEM) to assess solid bitumen composition and porosity development as a function of solid bitumen texture and association with minerals. A series of hydrous pyrolysis experiments (1-103 days, 300-370°C) using a low maturity (0.25% solid bitumen reflectance, BRo), high total organic carbon [(TOC), 14.0 wt. %] New Albany Shale sample as the starting material yielded pyrolysis residues designed to evaluate the evolution of TOC, solid bitumen aromaticity, and organic porosity development with increasing temperature and heating duration. Solid bitumen was analyzed by Raman spectroscopy wherein point data was collected from accumulations...
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For sample mounting, organic petrology laboratories typically use cold-setting epoxy-resin (e.g., 40°C, used by Oklahoma Geological Survey, OGS) or heat-setting plastic (e.g., 180°C, used by U.S. Geological Survey, USGS). Previous workers have suggested a systematic vitrinite reflectance (VRo) increase was associated with the thermoplastic preparation process, relative to epoxy mounting, which was attributed to moisture loss from the transient high temperatures of plastic mounting. In this study, we evaluated thermal effects to low maturity organic matter from transient exposure to elevated temperatures. A subbituminous coal sample was subjected to long-term (4 to 38 weeks) exposure to temperatures of 85 to 120°C...
The USGS Energy Resources Program (ERP) addresses the challenge of increasing demand for energy sources by conducting basic and applied research on geologic energy resources and on the environmental, economic, and human health impacts of their production and use. The ERP provides reliable and impartial scientific information on geologically based energy resources, including: oil, natural gas, coal, coalbed methane (CBM), gas hydrates, geothermal resources, uranium, oil shale, and bitumen and heavy oil. The Energy Resources Program is also involved in studying the impacts of wind and solar energy development. This community will serve as a primary footprint for Energy Resources Program products, projects, datasets,...


    map background search result map search result map Sample mounting for organic petrology: no thermal effects from transient exposure to elevated temperatures (2019) Textural occurrence and organic porosity of solid bitumen in shales Reflectance measurements for eight samples submitted to the USGS Organic Petrology Laboratory in Reston Textural occurrence and organic porosity of solid bitumen in shales Reflectance measurements for eight samples submitted to the USGS Organic Petrology Laboratory in Reston Sample mounting for organic petrology: no thermal effects from transient exposure to elevated temperatures (2019)