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An analytical method for the identification of eight plant phytoestrogens (biochanin A, coumestrol, daidzein, equol, formononetin, glycitein, genistein and prunetin) in soy products and wastewater samples was developed using gas chromatography coupled with ion trap mass spectrometry (GC/MS–MS). The phytoestrogens were derivatized as their trimethylsilyl ethers with trimethylchlorosilane (TMCS) and N,O-bis(trimethylsilyl)trifluoroacetamide (BSTFA). The phytoestrogens were isolated from all samples with liquid–liquid extraction using ethyl acetate. Daidzein-d4 and genistein-d4 labeled standards were used as internal standards before extraction and derivatization. The fragmentation patterns of the phytoestrogens were...
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This dataset consists of 262 variables which describe various known and suspected point and non-point sources of contaminants and endocrine disrupting compounds (EDCs) throughout the Chesapeake Bay Watershed. Contaminant data was summarized to the NHDPlus Version 2.1 catchment level (1:100K). Contaminant data summarized span a time range of 2001 to 2016 and include regulated facilities, pesticides, manure and biosolids application data, mercury deposition, animal feeding applications, septic systems, landfills, and land use and land cover. These data are presented in a comma separated file, which includes all variables summarized and the NHDPlus Version 2.1 FEATUREID field (also known as COMID). The FEATUREID field...
Categories: Data, Data Release - Revised; Types: Citation; Tags: Aquatic Biology, Chesapeake Bay, Chesapeake Bay Basin, Delaware, Discharge Monitoring Report (DMR), All tags...


    map background search result map search result map Potential contaminant sources and other landscape variables summarized for NHDPlus Version 2.1 catchments within the Chesapeake Bay Watershed (ver. 2.0, June 2021) Potential contaminant sources and other landscape variables summarized for NHDPlus Version 2.1 catchments within the Chesapeake Bay Watershed (ver. 2.0, June 2021)