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Over 300 samples were collected in New York, Vermont, and Massachusetts from wastewater treatment facilities (20 locations), drinking water facilities (9 locations), streams (53 locations), lakes (2 locations), a bay (1 location), and a POCIS (Polar Organic Chemical Integrative Sampler) blank sample between April 2009 and October 2018. This data release provides chemistry data for over 400 analytes, including pharmaceuticals, hormones, personal care and domestic use compounds, pesticides and other compounds using 10 different laboratory analytical methods on water, sediment, wastewater sludge, and POCIS samples. Quality assurance data, such as equipment and field blank data and percent recovery for isotopic dilution...
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This dataset contains the trace element concentration results for samples collected from tapwater sites in East Chicago, Indiana, August-September, 2017, and Chicago, Illinois, July-December, 2017. Samples were collected one time, from 45 private residences and associated drinking water plants and source water locations. Water-quality samples were analyzed at two U.S. Geological Survey laboratories: National Water Quality Laboratory, Denver, Colorado and at the Redox Chemistry Laboratory, Boulder, Colorado.
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Water-quality samples were collected at 49 surface water sites covering a range of land uses across the state of Iowa starting the summer of 2022 and continuing into the spring of 2023 by staff from the U.S. Geological Survey Central Midwest Water Science Center. Samples were submitted to the National Water Quality Laboratory in Denver, Colorado, and were analyzed for 32 per- and polyfluoroalkyl substances. Additional samples for N-(1,3-Dimethylbutyl)-N’-phenyl-p-phenylenediamine (6PPD) and 6PPD-Quinone were sent from a subset of the sites to the Organic Geochemistry Research Laboratory in Lawrence, Kansas.
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Nitrapyrin is a nitrification inhibitor that is co-applied with N-fertilizer in agroecosystems. Over the course of one year (March 2016 to June 2017), 192 water samples from seven streams across Iowa and Illinois were analyzed for nitrapyrin, its degradate 6-chloropicolinic acid (6-CPA), and three widely used herbicides acetochlor, atrazine, and metolachlor. Additional environmental samples were collected and analyzed in spring 2017: 63 water samples from eight subsurface drains, and 33 soil samples from a field in Iowa that received direct application of nitrapyrin (only for nitrapyrin and herbicides). Nitrapyrin was detected in all seven streams (56% detection) with concentrations ranging from 4 to 1,200 ng/L;...
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Dataset includes continuous discharge at the USGS (Station ID: 05485605) Fourmile Creek near Ankeny, IA DS1 gage site (http://waterdata.usgs.gov/usa/nwis/uv?site_no=05485605) as well as daily precipitation and water level data in select groundwater piezometers recorded in 10 minute intervals during the period Oct 1, 2013 to November 30 2013. Latitude and longitude data are provided for groundwater piezometer locations. This data release supports the following publication: Hubbard, L.E., S.H. Keefe, D.W. Kolpin, L.B. Barber, J.W. Duris, K.J. Hutchinson, and P.M. Bradley. Hydrologic Impact of Wastewater Contribution to Shallow Groundwater: Before and After Wastewater Discharge Cessation. Environmental Science: Water...
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This study focuses on providing a broad-scale assessment of composition of water chemistry in urban stormwater runoff. The stormwater runoff is a source of recharge to groundwater by Green Infrastructure (GI) practices or it may become a source of recharge to groundwater to reduce stormwater volumes to surface waters or augment groundwater supply. The chemical composition of the stormwater runoff is important to understanding the potential impacts of surface water recharge to groundwater. In this study, 21 field sites were sampled for stormwater runoff during 50 storm events from 7/28/2016 through 12/8/2017. Major elements were measured by inductively coupled plasma-optical emission spectrometry and trace elements...
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Chemical and microbiological results, quality assurance and quality control, site location, and method information for surface water, bed sediment, and wastewater effluent collected from 34 stream locations across Iowa (United States). Environmental samples were analyzed for a suite of 29 antibiotics, plated on selective media for 15 types of bacteria growth, and DNA was extracted from culture growth and used in downstream polymerase chain reaction (PCR) assays for the detection of 24 antibiotic resistance genes. Environmental field data were collected in-situ for water temperature (°C), specific conductivity (µs/cm), dissolved oxygen (mg/L), pH (standard units), and turbidity (FNU) using a multiparameter sonde...
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The Ankeny, Iowa wastewater treatment facility (WWTF) was decommissioned in November 2013 providing a unique opportunity to characterize the impacts of WWTF discharge on water quality at the surface-water/groundwater interface in a shallow, unconfined alluvial aquifer. The Ankeny WWTF discharged treated effluent for nearly forty years into Fourmile Creek, located in Ankeny, Iowa. Dataset includes site information (Table 1), analytical methods (Table 2), piezometer water level elevations (Table 3), trace and major element concentrations collected from 2011 to 2013 before the WWTF shutdown (Table 4), and trace and major element concentration collected from 2013 to 2014 after the WWTF shutdown (Table 5).
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Data were collected at 60 surface water and two effluent sites across Iowa in 2019-2020 by staff from the U.S. Geological Survey Central Midwest Water Science Center. Samples were submitted to the National Water Quality Laboratory in Denver, Colorado, and were analyzed for per- and polyfluoroalkyl substances.
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Spatial reconnaissance of fluvial microcystins (MC) concentrations and select water-quality parameters, including nutrients and periphyton biomass, in 75 wadeable streams in the Piedmont region of the southeastern USA during 2014. Data set includes only those data specifically discussed in the associated journal article: Loftin, K.A., Clark, J.M., Journey, C.A., Kolpin, D.W., Van Metre, P.C., and Bradley, P.M., 2016, Spatial and temporal variation in microcystins occurrence in wadeable streams in the southeastern USA: Environmental Toxicology & Chemistry, http://dx.doi.org/10.1002/etc.3391.
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Four dichloroacetamide herbicide safeners (AD-67, benoxacor, dichlormid, and furilazole) and two co-applied herbicides (acetochlor and metolachlor) were measured in water samples from 7 streams across Iowa and Illinois. Iowa water samples were collected from March 2016 to June 2017, and Illinois water samples were collected from September 2016 to June 2017. The compounds studied are applied to corn, and Iowa and Illinois are the two largest corn producing states in the U.S. The seven stream sites are all adjacent to agricultural fields in corn production. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. With the exception of one site, Iowa River at Wapello (USGS...
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The USGS conducted a combined wastewater facility pre/post-closure groundwater assessment adjacent to an effluent-impacted reach of Fourmile Creek, Ankeny, Iowa, USA. This data release includes pharmaceutical concentration data for Fourmile Creek determined by enzyme-linked immunosorbent assay (ELISA) and HPLC-MS/MS during the period October 2012 to October 2014, along with associated HPLC-MS/MS analyte and method performance information.
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In the United States and globally, contaminant exposure in unregulated private-well point-of-use (POU) tapwater (TW) is a recognized public health data gap and an obstacle to both risk management and homeowner decision making. To help address the lack of data on broad contaminant exposures in private-well TW from hydrologically vulnerable (alluvial or karst) aquifers in agriculturally intensive landscapes, samples were collected in 2018-2019 from 47 northeast Iowa farms and analyzed for 437 unique organic compounds, 32 inorganic constituents, 5 in vitro bioassays, and 11 microbial assays.
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Oklahoma State University South-Central Research Station (SCRS) was used to conduct research to understand the chemical composition of various water types and their potential environmental and human health effects. The study area provided the opportunity to study five water types: (1) receiving surface water (Washita River), (2) urban stormwater, (3) wastewater treatment plant effluent used for irrigation, (4) rain-induced runoff from an effluent-irrigated cornfield, and (5) rain-induced runoff from a dryland cornfield. Fifteen water samples were collected from August 2018 to October 2019. In addition, two composite above ground whole-corn plant samples (i.e., stem, leaves, grain) were collected from the effluent...
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Samples were collected, processed, and analyzed for organics, estrogen equivalents, and fecal indicator bacteria. Filtered organic samples were sent to the National Water Quality Laboratory in Denver, Colorado. Unfiltered estrogen equivalent samples were sent to the Organic Geochemistry Research Lab in Lawrence, Kansas, for extraction, after which they were sent to the National Fish Health Research Laboratory in Leetown, West Virginia. Bacteria samples were processed at the Central-Midwest Water Science Center Iowa City, Iowa, office. Staff collected field parameters in-situ.
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This data release presents chemical and biological results from investigations of water quality, fish endocrine disruption, and emergent insects in the Shenandoah River Watershed (Virginia and West Virginia, USA) conducted during 2014, 2015, and 2016. Multiple sampling campaigns were conducted at sites located throughout the Shenandoah River Watershed (Table 1). The complex inorganic and organic chemical characteristics of river waters and wastewater treatment plant effluents were characterized using 21 separate analytical methods at 7 laboratories (Tables 2, 3, and 4). To assess the relations between water composition and fish endocrine disruption, 21-day mobile laboratory adult fathead minnow exposure experiments...
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Nitrapyrin, a nitrification inhibitor, 6-CPA, a nitrapyrin degradate, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in surface drains from eights sites in Illinois. Water samples were collected from April to June 2017. The compounds studied are applied to corn, Illinois is one of the largest corn producing states in the U.S. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. Water samples were filtered (0.7 micrometers), extracted via solid phase extraction (Oasis® MAX cartridge), and analyzed (nitrapyrin and herbicides by gas chromatography with mass-spectrometry; 6-CPA by liquid chromatography tandem mass-spectrometry).
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Nitrapyrin, a nitrification inhibitor, 6-CPA, a nitrapyrin degradate, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in water samples from seven streams across Iowa and Illinois. Iowa water samples were collected from March 2016 to June 2017, and Illinois water samples were collected from September 2016 to June 2017. The compounds studied are applied to corn, and Iowa and Illinois are the two largest corn producing states in the U.S. The seven stream sites are all adjacent to agricultural fields in corn production. Water samples (1-L) were collected in amber glass bottles using a grab or depth weighted approach. With the exception of one site, Iowa River at Wapello (USGS Site...
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Nitrapyrin, a nitrification inhibitor, and three co-applied herbicides (acetochlor, atrazine, and metolachlor) were measured in soil samples from an agricultural field in Iowa. Samples were collected from three locations in the field before and after nitrapyrin application in April-May 2017. Soils were collected using a 5-inch pipe that was hammered into the ground. Soil samples were extracted using pressurized solvent extraction (with dichloromethane), clean-up via solid phase extraction (carbon and alumina sorbents), and analyzed by gas chromatography with mass-spectrometry.
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This data set contains the result for inorganic constituents and organic compounds collected from tapwater locations, as well as water filtration plants, in East Chicago, Indiana, and Chicago, Illinois in 2017. Additionally quality assurance data collected was summarized. Residential samples collected were done so directly from residential kitchen taps (faucets) as is, it was noted if a point-of-use filtration device was utilized by the homeowner, but they were not removed for sampling. Samples were collected at various times of the day, without regard to previous water use. Results were analyzed using ToxCast, and Exposure Activity Ratios (EARs) are presented. Water filtration plant samples were taken from Lake...


map background search result map search result map Periphyton (1993-2011) and Water Quality (2014) Data for ET&C Article Entitled Spatial and Temporal Variation in Microcystins Occurrence in Wadeable Streams in the Southeastern USA Precipitation, surface-water discharge, and groundwater elevation data for Fourmile Creek, Ankeny, Iowa, USA during October 1, 2013 to November 30, 2013 Concentrations and associated method information for pharmaceutical contaminants analyzed in Fourmile Creek near Ankeny, Iowa, USA during the October 2012 to October 2014 wastewater treatment facility pre/post-closure assessment Concentrations and associated method information for trace and major elements in Fourmile Creek near Ankeny, Iowa, USA during the 2011-2014 wastewater treatment facility pre/post-closure assessment Herbicide Safener and Co-Applied Herbicide Concentrations for Seven Streams across Iowa and Illinois (March 2016 to June 2017) Assessment of Endocrine Disruption in the Shenandoah River Watershed – Chemical and Biological Data from Mobile Laboratory Fish Exposures and Other Experiments Conducted during 2014, 2015, and 2016 Occurrence and Concentrations of Trace Elements in Discrete Tapwater Samples Collected in Chicago, Illinois and East Chicago, Indiana, 2017 Nitrapyrin, 6-CPA, and herbicide concentrations in agricultural soils, subsurface drains, and corresponding streams in the Midwestern US Nitrapyrin, 6-CPA, and herbicide concentrations in streams in the Midwestern US (March 2016 to June 2017) Nitrapyrin, 6-CPA, and herbicide concentrations in subsurface drains in the Midwestern US (April 2017 to June 2017) Nitrapyrin and herbicide concentrations in soil in the Midwestern US (April 2017 to May 2017) Survey of major and trace elements in stormwater runoff from across the United States, 2016 to 2017 Mixed Organic and Inorganic Tapwater Results in the Greater Chicago Area, USA, 2017-2019 Water-quality data for a pharmaceutical study at Muddy Creek in North Liberty and Coralville, Iowa, 2017-2018 Target-Chemical Concentrations, Exposure Activity Ratios, and Bioassay Results for Assessment of Mixed-Organic/Inorganic Chemical Exposures in Northeast Iowa Private-Well Tapwater, 2018 Water-quality data for a statewide assessment of per- and polyfluoroalkyl substances (PFAS) study in Iowa, 2019-2020 Water-quality results from a wastewater reuse study: Inorganic and organic compositions of wastewater effluent and select urban and agricultural water types during rain-induced runoff, Chickasha, Oklahoma, 2018-2019 Emerging contaminant data at wastewater treatment facilities, municipal water supplies, surface water and lake sites in the northeastern United States, 2009-2018 (ver. 1.1, January 2023) Antibiotic and Antibiotic Resistance Signatures in Iowa Streams, 2019 State-Wide Reconnaissance of Per- and Polyfluoroalkyl Substances, N-(1,3-Dimethylbutyl)-N-phenyl-p-phenylenediamine (6PPD), and 6PPD-Quinone in Iowa Streams, 2022-2023 Concentrations and associated method information for pharmaceutical contaminants analyzed in Fourmile Creek near Ankeny, Iowa, USA during the October 2012 to October 2014 wastewater treatment facility pre/post-closure assessment Precipitation, surface-water discharge, and groundwater elevation data for Fourmile Creek, Ankeny, Iowa, USA during October 1, 2013 to November 30, 2013 Water-quality data for a pharmaceutical study at Muddy Creek in North Liberty and Coralville, Iowa, 2017-2018 Concentrations and associated method information for trace and major elements in Fourmile Creek near Ankeny, Iowa, USA during the 2011-2014 wastewater treatment facility pre/post-closure assessment Mixed Organic and Inorganic Tapwater Results in the Greater Chicago Area, USA, 2017-2019 Occurrence and Concentrations of Trace Elements in Discrete Tapwater Samples Collected in Chicago, Illinois and East Chicago, Indiana, 2017 Assessment of Endocrine Disruption in the Shenandoah River Watershed – Chemical and Biological Data from Mobile Laboratory Fish Exposures and Other Experiments Conducted during 2014, 2015, and 2016 Target-Chemical Concentrations, Exposure Activity Ratios, and Bioassay Results for Assessment of Mixed-Organic/Inorganic Chemical Exposures in Northeast Iowa Private-Well Tapwater, 2018 Nitrapyrin and herbicide concentrations in soil in the Midwestern US (April 2017 to May 2017) Nitrapyrin, 6-CPA, and herbicide concentrations in subsurface drains in the Midwestern US (April 2017 to June 2017) Water-quality data for a statewide assessment of per- and polyfluoroalkyl substances (PFAS) study in Iowa, 2019-2020 Antibiotic and Antibiotic Resistance Signatures in Iowa Streams, 2019 State-Wide Reconnaissance of Per- and Polyfluoroalkyl Substances, N-(1,3-Dimethylbutyl)-N-phenyl-p-phenylenediamine (6PPD), and 6PPD-Quinone in Iowa Streams, 2022-2023 Water-quality results from a wastewater reuse study: Inorganic and organic compositions of wastewater effluent and select urban and agricultural water types during rain-induced runoff, Chickasha, Oklahoma, 2018-2019 Herbicide Safener and Co-Applied Herbicide Concentrations for Seven Streams across Iowa and Illinois (March 2016 to June 2017) Nitrapyrin, 6-CPA, and herbicide concentrations in agricultural soils, subsurface drains, and corresponding streams in the Midwestern US Nitrapyrin, 6-CPA, and herbicide concentrations in streams in the Midwestern US (March 2016 to June 2017) Periphyton (1993-2011) and Water Quality (2014) Data for ET&C Article Entitled Spatial and Temporal Variation in Microcystins Occurrence in Wadeable Streams in the Southeastern USA Emerging contaminant data at wastewater treatment facilities, municipal water supplies, surface water and lake sites in the northeastern United States, 2009-2018 (ver. 1.1, January 2023) Survey of major and trace elements in stormwater runoff from across the United States, 2016 to 2017