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Data in this data release were obtained for water samples collected under Yellowstone National Park Research Permit YELL-05194 in 2017 through the Integrated Yellowstone Studies Project funded by the Mineral Resources Program. Isotope-spiked incubations were carried out to determine methylation and demethylation potential for Frying Pan spring, Crystal Sister East, Crystal Sister West, and Turbulent Pool, which were selected based on existing data on total mercury and methylmercury concentrations (see companion data release (https://doi.org/10.5066/P9IUY03O). The data represent the experimental conditions of incubation experiments (temperature, time, and experimental spikes) and concentration data associated with...
This dataset describes mercury (Hg) stable isotope values in fish dorsal muscle from different freshwater environments across the globe. Fish were collected at numerous field sites in North America, South and Central America, Africa, and Asia from 2006-2020. Sub-samples were provided by cooperators to the U.S. Geological Survey Mercury Research Laboratory and the University of Wisconsin for mercury stable isotope analysis. Samples were analyzed for mercury stable isotopes from 2017-2021. These specimens represent multiple trophic levels and body sizes from different food webs and when adequate mass was available, multiple species from the same food web were examined. Cooperators include, but are not limited to:...
This data release includes mercury concentrations and mercury stable isotope measurements measured in sediments and biological tissues collected from the Saint Louis River located in Minnesota. Sediments and biota were collected by the U.S. Geological Survey, U.S. Environmental Protection Agency, U.S. Army Corps of Engineers, and federal contractors (Battelle) from 2017-2021. Collection regions included nearshore zones within the main estuary, remedial sites within the lower river, and upstream reservoir sites. Sediments were analyzed for total mercury, methylmercury, and mercury stable isotopes by the U.S. Geological Survey Mercury Research Laboratory (MRL, Madison, Wisconsin). Biological samples were analyzed...
Categories: Data;
Tags: Environmental Health,
Geochemistry,
Saint Louis River, Minnesota,
USGS Science Data Catalog (SDC),
biota,
This dataset consists of concentration and isotopic data for a method designed to isolate and analyze methylmercury. Several matrices (lab-based, and natural) were tested to ensure that the method was capable of recovering methylmercury amendments. Additionally, natural matrices (plankton and sediment) with ambient methylmercury were also analyzed to ensure that the method could be successfully applied to natural matrices. Separation tests for sediment, water, and biotic matrices showed acceptable recoveries (98 ± 5%, n = 54) and reproducible δ202Hg isotope results (2SD < 0.15 ‰) down to 5 ng of MeHg. This dataset is part of a complimentary paper published in Analytical and Bioanalytical Chemistry (https://doi.org/10.1007/s00216-019-02277-0)...
Categories: Data;
Tags: Environmental Health,
Fox River, WI,
Geochemistry,
Lake Mendota, WI,
Lake Michigan,
Water quality and fish tissue samples were collected and measured for mercury concentrations in a total of 23 small to medium size lakes in Minnesota to assess the impact that zebra mussel (Dreissena polymorpha) invasion had on mercury bioaccumulation. Water samples were collected in October and November of 2021 from 22 lakes and analyzed for total mercury, methylmercury, dissolved organic carbon, and suspended particulate matter at the U.S. Geological Survey (USGS) Mercury Research Laboratory (MRL). Tissue samples of walleye (Sander vitreus) and yellow perch (Perca flavescens) were collected by researchers at the University of Minnesota, Twin Cities from July to October in 2019 and 2021 and June to October in 2020...
Categories: Data;
Tags: Aquatic Biology,
Environmental Health,
Minnesota,
USGS Science Data Catalog (SDC),
Water Quality,
This dataset includes field hydrologic measurements and laboratory analyses of surface and pore waters, sediments, benthic plants/biofilms, and biota along the Middle Snake River upgradient of the Hells Canyon Complex. The study region for this work focuses on a section of the Snake River heavily utilized for agriculture, with complex systems of irrigation diversion and return drainage, spanning 164 km above the Hells Canyon Complex (Idaho, Oregon). The goal of this study was to identify potential loading sources of methylmercury from the upgradient Snake River into the reservoir complex, with a focus on the tributaries, irrigation return drains, and riparian zones adjacent to agricultural lands along the river....
Methylmercury (MeHg) and total mercury (HgT) stable isotope measurements were made by the USGS Mercury Research Lab (MRL) in different organs on the Giant Petrels (Macronectes spp.) to examine internal mercury cycling in these seabirds. These data were collected as a compliment to x-ray spectroscopy measurements made by the University of Grenoble, France. The tissues and feathers of the southern giant petrels exhibit large variability in mercury-202 isotope values (δ202HgT), which are typically used to ascertain Hg sources in the environment. These values follow a pattern across all individuals based on tissue type: feathers (δ202HgT = 2.74 ± 0.16‰, n =5, mean ± standard deviation) > brain (δ202HgT = 1.09 ± 0.77‰,...
Categories: Data;
Tags: Antarctica,
Ecology,
Geochemistry,
Kerguelen Islands,
USGS Science Data Catalog (SDC),
The data in this data release includes results from the analysis of water and fish from 76 sites in the Everglades National Park (ENP). Water and particulate matter samples were collected from 2008 to 2018 and analyzed for total mercury (THg) and methylmercury (MeHg). Filtered water samples were also analyzed for dissolved organic carbon (DOC), specific ultraviolet absorbance (SUVA), and major anions. Fish samples (Eastern Mosquitofish, Flagfish, African Jewelfish, Golden Topminnow, and Mayan Cichlid species) were collected from 2007 to 2018 and analyzed for THg and MeHg and carbon and nitrogen stable isotopes. These data are important for analyzing hydrologic and geochemical controls on MeHg distribution and production...
Categories: Data;
Tags: Environmental Health,
Everglades National Park,
Fish,
Geochemistry,
Mercury Contamination,
Fish collected for taxonomic and systematic purposes are often preserved and then archived in museum collections. Preserved fish are commonly first fixed in a formalin solution and then transferred to ethanol for long-term storage. The wet preservation method can potentially introduce mercury (Hg) contamination or unintentionally extract Hg from tissue. An experiment was designed to test the utility of museum preserved fishes in reconstructing spatiotemporal trends in methylmercury (MeHg) concentration and Hg stable isotope ratios, which is used to trace Hg sources to fishes. Wet preserved fish specimens from the Congo River and river basins within Gabon were subsampled from archives at the the Royal Museum of Africa...
Categories: Data;
Tags: Congo,
Environmental Health,
Gabon,
Minamata Convention,
USGS Science Data Catalog (SDC),
This data relates to the development of a modified pre-concentration method for mercury (Hg) stable isotope measurements that uses chemical Hg reduction and gold trap amalgamation followed by semi-rapid thermal desorption (less than 1 hour) and chemical trapping in a novel oxidizing solution. The thermal desorption method was demonstrated to perform adequately on multiple trapping matrices previously presented, however our new bromine monochloride (BrCl) wet oxidant trap (40% 3HNO3:BrCl) was deemed superior. As such, this solution was capable of trapping consistently in 2mL volume over a wide range of Hg masses (5 to 200 ng). The procedure was also shown to work effectively on natural matrices, waters and sediments,...
The dataset presented here represents the concentrations and stable isotopic composition of gaseous mercury (Hg) for 31 sites across the United States. This national-scale monitoring effort was performed by the National Atmospheric Deposition Program (NADP) and the USGS over a two-year period (March 2016 - May 2018). The network includes a highly diverse set of sites ranging from remote (e.g. Denali National Park, AK and Mauna Loa, HI) to highly urbanized (e.g. Bronx, NY and Boston, MA). Air samples were collected using a custom designed bulk air sampler, in which air was pumped at approximately 1 L/min through particulate and soda lime filters prior to passing through two quartz tubes containing gold coated glass...
Categories: Data;
Tags: Bad River, WI,
Boston, MA,
Bronx, NY,
Clifty Falls State Park, IN,
Consumnes River, CA,
The St Louis River (SLR) is the second largest tributary to Lake Superior and a designated area of concern (AOC) due to past industrial contamination of organic chemicals and heavy metals, including mercury (Hg). Sediments, prey items (odonates, mixed benthic invertebrates, and spiders), and game fish were targeted within this study to determine if industrial sources of Hg were bioaccumulating into the food web. Samples from SLR were directly compared to a reference site in the Bad River, WI to assess if legacy contamination resulted in elevated Hg concentrations in comparisons to background regions with no known point sources. Carbon and nitrogen isotopes were also employed as food web tracers to determine if dietary...
Categories: Data;
Tags: Bad River, WI,
Environmental Health,
Geochemistry,
Lake Superior,
St Louis River, MN,
This dataset includes laboratory analyses of surface water samples and sediment trap material collected from (1) locations upstream, downstream, and within the Hells Canyon Complex (Idaho, Oregon) of the Snake River, (2) tributaries of the Snake River, and (3) two reservoirs near Boise, Idaho, from 2014 to 2022. The study area spans approximately 232 river miles of the Snake River and includes: two sites on the main stem of the Snake River upstream of the Hells Canyon Complex (Snake River mile 447.6, 399.0, and 345.6), six sites within Brownlee Reservoir (Snake River mile 318, 314, 310, 305, 300, and 286), one site within Oxbow Reservoir (Snake River mile 273), two sites within Hells Canyon Reservoir (Snake River...
The lower Fox River in Wisconsin is a heavily industrialized system and the major tributary to Green Bay within Lake Michigan. The region has been a listed as Area of Concern by the United States Environmental Protection Agency (USEPA), indicating severe impairment of the ecological health of the system. Remedial action has taken place along the river to remove extensive polychlorinated biphenyl (PCB) contamination. However, it was unknown if mercury (Hg), also derived from industrial activity, remained within sediments and actively bioaccumulated within the food web. Mercury stable isotopes were analyzed in sediments and waters collected below the DePere Dam and upstream at Lake Winnebago to compare if Hg sources...
Categories: Data;
Tags: Environmental Health,
Fox River, WI,
Geochemistry,
Green Bay,
Lake Michigan,
The Hannibal Pool of the Ohio River is heavily industrialized and receives direct effluent discharges from coal power plants, chlor-alkali plants, and sewage treatment facilities. Mercury (Hg) is a contaminant of concern due to the risk of bioaccumulation at wildlife refuges also located within this region. Mercury concentrations and isotopes compositions were measured to assess the levels and source of Hg contamination, respectively within the system. Sediments and waters were measured to define isotopic end members within Hannibal Pool. Heelsplitter mussels, zebra mussels, and prey fish were also analyzed to determine if Hg source signatures were conserved within the food web. These data are a part of a larger...
Categories: Data;
Tags: Ecology,
Geochemistry,
Hannibal Pool,
Ohio River,
USGS Science Data Catalog (SDC),
Samples were collected from Clear Lake, California from 2019-2022 by the U.S. Geological Survey (USGS) California Water Science Center, the USGS Forest and Rangeland Ecosystem Science Center (FRESC), the US Environmental Protection Agency, and EA Engineering Science and Technology Inc. to assess the extent and cycling of legacy mercury (Hg) contamination from Sulphur Bank Mine. Samples of waste rock, sediments, groundwater, and biological tissue (zooplankton, bluegill, smallmouth bass, Mississippi silversides, and largemouth bass) were analyzed for Hg stable isotopes by the U.S. Geological Survey Mercury Research Laboratory. Mercury concentrations for sediments, waste rocks, and groundwaters are included within...
Categories: Data;
Tags: California,
Clear Lake, California,
Environmental Health,
Lake County, California,
USGS Science Data Catalog (SDC),
Comma-separated values (.csv) file containing data related to mercury in Salmonid fishes collected from the Snake River and tributaries, Idaho and Oregon.
The Northeast Stream Quality Assessment (NESQA) performed mercury (Hg) isotope analysis of prey fish, game fish, and sediments from 29 sites across an urban to forested land-use gradient. The data presented here includes the chemical analysis of Hg concentrations and isotopes, capture information for fish species, land use, and stream water quality variables. Using these parameters it was determined that the preservation of Hg isotope signatures, which are indicative of source (e.g. atmospheric deposition, industrial point discharge), were dependent on land use, proximity to point sources, and variables related urbanization (e.g. road density and impervious surface cover). Additional Information regarding the interpretation...
Categories: Data;
Tags: Connecticut,
Massachusetts,
New Hampshire,
New York,
Northeast United States,
As part of the larger Great Lakes Sediment Surveillance Program (GLSSP), the U.S. Geological Survey Mercury Research Laboratory (MRL) partnered with the U.S. Environmental Protection Agency and the University of Minnesota-Duluth to assess contaminant concentrations within surface sediments and sediment cores from the Laurentian Great Lakes. Sediments were assessed for mercury concentrations and mercury stable isotopes to examine spatial trends and sources of mercury within the lakes. In 2021, 30 sites were surveyed in Lake Superior. Mercury concentrations within Lake Superior surface sediment ranged from 1.1 to 161.2 ng/g. Mercury isotopes displayed a range in δ202Hg from -0.12 to -1.74 ‰ with measurable Δ199Hg...
This study was designed to examine mercury (Hg) stable isotope values in filtered water and suspended particulate matter from tributaries to the Snake River located in Oregon and Idaho. Water samples were collected from 21 tributary sites representing a range of watershed land use types (e.g., agriculture, forest, etc.) within the Snake River Basin. In 2018, water samples were collected at tributary sites near the confluence of the Snake River and at sites upstream higher in the watershed. In the 2019 and 2020, the tributary water sample collection was focused on downstream sites near the Snake River. In addition, from 2015-2018 Hg stable isotopes were also measured in air, bed sediment, and geologic material from...
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