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Neonicotinoids have become the most widely used insecticides in world with rapid growth in applications as seed coatings. Nontarget organisms are exposed to concentrated levels of pesticidal active ingredients through ingestion of treated seeds. To better understand pesticide fate, analytical methods are necessary to rapidly screen and accurately quantitate contaminants in environmental and biological matrices. Liquid chromatography-tandem mass spectrometry (LC-MS/MS) is commonly employed for neonicotinoid analyses but requires expensive analytical instrumentation and potentially laborious sample preparation. Enzyme-linked immunosorbent assays (ELISAs) are efficient and sensitive alternative methods for neonicotinoid...
Categories: Data;
Tags: Coturnix japonica,
Environmental Health,
USGS Science Data Catalog (SDC),
United States,
environment,
This data release contains the concentration and quality-assurance results for inorganic constituents, as well as organic compounds (volatile organic compounds [VOC], per- and polyfluoroalkyl substances [PFAS], pesticides and disinfection byproducts [DBP]) and microbiological results collected in the Little Big Horn River and residential or commercial tapwater locations in Montana. Twenty-two tapwater samples (six sourced from public supply and 14 sourced from private wells) and six surface-water samples were collected in Montana between August 8-10, 2022. Pharmaceuticals, VOC, and PFAS were analyzed at the U.S. Geological Survey (USGS) National Water Quality Laboratory (NWQL) in Denver, Colorado. Pesticides and...
Categories: Data;
Tags: Environmental Health,
Montana,
USGS Science Data Catalog (SDC),
United States,
Water Quality,
These data present chemistry and toxicity results from freshwater stream sediments collected from 99 wadable stream sites across eleven states in the Midwestern U.S. as one component of a larger USGS study in the summer of 2013. This data presents a selected suite of chemistry collected at these sites (PAHs, Organochlorines, PCBs, Trace Elements, and current use pesticides) used in calculating a Probable Effect Concentration-Likely Effect Benchmark quotient mixture score for contaminants measured in sediments. The toxicity data presents results of toxicity tests following ASTM and US EPA standard methods for sediment toxicity tests with the amphipod Hyalella azteca (28-d exposure), the midge Chironomus dilutus (10-d),...
Irrigation runoff and soil samples were collected from a lettuce field located at the USDA-ARS Spence Research farm in the Salinas Valley, California to measure neonicotinoid insecticides (clothianidin and imidacloprid) and a fungicide (azoxystrobin) applied via coated seed and drench treatments. The field trial was designed to evaluate four treatments with replication: 1) control, untreated seed, 2) imidacloprid treated seed, 3) clothianidin treated seed, and 4) azoxystrobin treated seed with an imidacloprid drench. Samples were collected from each treatment over two lettuce growing seasons: August to October 2019 and September to October 2020. Runoff samples were collected over both growing seasons during 6 irrigation...
Categories: Data;
Tags: California,
Salinas,
Soil Sciences,
USGS Science Data Catalog (SDC),
Water Quality,
This data release includes sampling location data, field-collected wetland attribute data, field-collected water chemistry data, laboratory-processed water chemistry data (anions, cations, alkalinity, nutrients, chlorophyll a concentrations, dissolved organic carbon, and specific ultraviolet absorbance, pesticide concentrations), dry mass of adult aquatic insects emerging from the surface of the wetlands, taxonomic classifications of the insects collected, and whole-body pesticide concentrations for adult aquatic insects emerging from wadeable wetlands in cropland and grassland landscapes across a salinity/hydrology gradient (N = 14 wetlands in 2015, N = 15 wetlands in 2016). Sampling was completed in late spring,...
Zooplankton samples were collected at one site upstream of the Yolo Bypass in Northern California, three sites within the Bypass, and at a comparison site on the Sacramento River below the city of Sacramento and analyzed for a large suite of current-use pesticides and degradates. Samples were collected every two weeks from early August 2021 to mid-October 2021. Samples were collected by towing a 150-micron conical plankton net for 5 minutes by boat at each site. In the laboratory, zooplankton samples were filtered through a 63-micrometer sieve to separate the zooplankton and vegetation/detritus from the water. Large sticks, twigs, rocks, and leaves were rinsed with organic free water into the sieve and then discarded....
Categories: Data;
Tags: California,
Environmental Health,
Hydrology,
Sacramento,
USGS Science Data Catalog (SDC),
Hybrid sunflower production occurs near Sacramento in Northern California where seed treatments are commonly used. In this study, four locations were sampled in 2016 as matched pairs; half of each field was sown with thiamethoxam treated seed and half without. In addition to the thiamethoxam seed treatment, all seeds were coated with two fungicides, fludioxonil and mefenoxam/metalaxyl. Both wild bee and honey bee pesticide exposure was assessed by analyzing field soil, sunflower pollen and nectar, honey bees (pollen and nectar foraging) and a sunflower specialist wild bee, Melissodes agilis. Samples were extracted via pressurized liquid extraction (except nectar which underwent a room temperature solvent extraction)...
Categories: Data;
Tags: California,
Environmental Health,
USGS Science Data Catalog (SDC),
environment,
fungicides,
Analysis of biological tissues or direct sources of food may better characterize exposure of non-target organisms to current-use pesticides. Food boluses were collected from tree swallow (Tachycineta bicolor) nestlings using a non-lethal, ligature method and were composited based on nest. The ligatures, which prevented the bolus from being swallowed, were placed on nestlings for 1 h until samples were collected. Samples in 2016 were collected from nestlings at 6 days and 12 days post-hatch whereas 2018 samples were collected from nestlings at 12 days post-hatch. Furthermore, in 2016 and 2018, insects commonly consumed by tree swallows were collected via sweep net and composited based on suborder (Brachycera, Nematocera,...
Chemically intensive crop production depletes wildlife food resources, hinders animal development, health, survival, and reproduction, and it suppresses wildlife immune systems, facilitating emergence of infectious diseases with excessive mortality rates. Gut microbiota is crucial for wildlife’s response to environmental stressors. Its composition and functionality are sensitive to diet changes and environmental pollution associated with modern crop production. In the study entitled Exposure to crop production alters cecal prokaryotic microbiota, inflates virulome and resistome in wild prairie grouse we use shotgun metagenomics to demonstrate that exposure to modern crop production detrimentally affects cecal...
Water primrose (Ludwigia hexapetala) is an invasive aquatic plant that has rapidly increased in coverage throughout the Sacramento-San Joaquin Delta. Water primrose has invaded wetlands and may contribute towards mortality of tules (Schoenoplectus spp.) and cattails (Typha spp.). Little research has been completed on the mechanisms responsible for marsh loss, but previous studies have suggested that water primrose contains allelopathic chemicals that could cause plant mortality. Three major allelopathic polyphenols (myricitrin, prunin, and quercitrin) previously identified in L. hexapetala leaves were measured in leaf, water, and soil samples from Delta marshes infested with water primrose. Samples were collected...
The data include concentrations of current use pesticides in tissues of larval wood frog (Lithobates sylvaticus) and spotted salamander (Ambystoma maculatum) and the presence of ranavirus in wood frogs and spotted salamanders from three northeastern National Wildlife Refuges sampled in 2013 and 2014. The data also include estrogenicity, protein phosphatase 2A inhibition and a suite of 15 major and minor elements in sediment screened using portable X-Ray Fluorescence. The data include sediment and tissue samples collected from 16 wetlands at the Patuxent Research Refuge (PRR) in central Maryland, USA, 15 wetlands at the Assabet River and Oxbow National Wildlife Refuges (EMASS) in eastern Massachusetts, USA, and nine...
Nitrapyrin is a nitrification inhibitor that is co-applied with N-fertilizer in agroecosystems. Over the course of one year (March 2016 to June 2017), 192 water samples from seven streams across Iowa and Illinois were analyzed for nitrapyrin, its degradate 6-chloropicolinic acid (6-CPA), and three widely used herbicides acetochlor, atrazine, and metolachlor. Additional environmental samples were collected and analyzed in spring 2017: 63 water samples from eight subsurface drains, and 33 soil samples from a field in Iowa that received direct application of nitrapyrin (only for nitrapyrin and herbicides). Nitrapyrin was detected in all seven streams (56% detection) with concentrations ranging from 4 to 1,200 ng/L;...
In January 2024 adult monarch butterflies (Danaus plexippus (Linnaeus, 1758)) were found dead near their overwintering site in Pacific Grove, Monterey County, California, USA. Ten of the deceased monarchs (six females and four males) were collected from three sites by staff at the Pacific Grove Museum of Natural History and sent to the U.S. Geological Survey Organic Chemistry Research Laboratory for analysis. Each individual adult monarch was analyzed following methods in Black et al., 2023 and Gross et al., 2024a and 2024b for 181 pesticides and pesticide transformation products; 15 pesticides were detected and included 8 insecticides/insecticide transformation products, 2 fungicides, and 4 herbicides/herbicide...
A multiresidue method for solids (i.e., soil, sediment, sludge) was developed and evaluated for the analysis of pesticides and pesticide degradates. Initially, a well characterized soil was used to determine the recovery of target compounds using an Energized Dispersive Guided Extraction (EDGE) system with two extraction solvents, acetonitrile and 1:1 (v/v) hexane:acetone. Extracts were cleaned using solid-phase extraction (SPE) with graphitized carbon cartridges and three elution solvents, acetonitrile, dichloromethane, and 1:1 (v/v) dichlormethane:ethyl acetate. The individual SPE elutions from the two extraction solvents were analyzed separately via GC-MS/MS and LC-MS/MS for 210 pesticides and pesticide transformation...
Categories: Data;
Tags: Environmental Health,
USGS Science Data Catalog (SDC),
biosolids,
contaminant transport,
environment,
The data presented in this data release include concentrations of current-use pesticides, nutrients, chloride, and metals in surface water collected from 60 wetlands including natural ponds, excavated ponds (Xponds), and stormwater basins in the New Jersey Pinelands, 2018-20. Site information, basic water-quality parameters, and method information also are included.
In the spring of 2021, six households with private wells were selected throughout Graton, California, based on proximity to agriculture (within one mile of agriculture), well depth (i.e., less than 150 feet in depth), and well type (i.e., dug versus drilled). Silicone bands were deployed for 30 days at outdoor locations at each household to passively sample pesticides in ambient air. On May 3, 2021, the silicone bands were retrieved and outdoor water samples (i.e., spigot on the side of the house) and indoor tap water samples (i.e., kitchen faucet used for drinking water) were collected and analyzed for 187 pesticides, 57 potential hormonally active chemicals, and estrogenicity. This study was a citizen science...
Categories: Data;
Types: Map Service,
OGC WFS Layer,
OGC WMS Layer,
OGC WMS Service;
Tags: Environmental Health,
USGS Science Data Catalog (SDC),
Water Quality,
Water Quality
In the United States and globally, the lack of data on contaminant exposure from unregulated private-well point-of-use (POU) tapwater (TW) is a recognized public health data gap and an obstacle to risk management and homeowner decision making. Mead, Nebraska, is an agricultural community about 30 miles west of Omaha. To help address the lack of data on broad contaminant exposures in TW sourced from private water wells, a total of 22 samples were collected from 18 private wells during June 2022 and January 2023 and analyzed for 495 organic compounds, 34 inorganic constituents, and 11 microbial groups. The organic compounds included pesticides, pharmaceuticals, volatile organic compounds (VOCs), disinfection byproducts...
Categories: Data;
Types: Map Service,
OGC WFS Layer,
OGC WMS Layer,
OGC WMS Service;
Tags: Environmental Health,
Nebraska,
USGS Science Data Catalog (SDC),
Water Quality,
biota,
Surface water samples were collected from four stream/agricultural drain sites in the Sacramento Valley of California to measure pesticides commonly applied to rice. Samples were collected weekly from May through August 2010 to capture the rice pesticide application season. Water samples were filtered (0.7 µm) and extracted via solid-phase extraction. Additionally, the filter paper was solvent extracted to measure suspended sediment-associated pesticides. Both fractions were analyzed via gas chromatography-mass spectrometry. A total of 89 pesticides and pesticide degradates were measured in the dissolved water phase, while 14 pyrethroid insecticides were measured in the suspended sediment-associated fraction (pyrethroids...
Categories: Data;
Tags: California,
Environmental Health,
Sacramento Valley,
USGS Science Data Catalog (SDC),
Water Quality,
Water, sediment, anuran food (leaf litter and detritus) and whole body larval amphibian composites were analyzed for over 100 current-use pesticides from 24 wetlands representing land-use gradients in the New Jersey Pinelands, USA during 2014-2016. Emerging amphibian pathogens, Ranavirus and Batrachochytrium dendrobatidis (Bd) were also assessed in individual larvae at the 24 wetlands. Tables in this data release contain the results from these analyses, with quality assurance summaries, along with site information, including land-use classifications.
Categories: Data;
Tags: Aquatic Biology,
New Jersey,
Pinelands,
USGS Science Data Catalog (SDC),
Water Quality,
This dataset contains the concentration and quality assurance results for inorganic and organic analytes collected for the U.S. Geological Survey (USGS), Ecosystems Mission Area, Environmental Health Infrastructure Program, Tapwater Exposure Project conducted in Minnesota, in August of 2019. Samples were obtained from multiple publicly distributed water sources in Minnesota in 2019. Due to privacy concerns, the exact location where samples were collected are not reported and station identification numbers have been anonymized. Water-quality samples were analyzed for pesticides, pharmaceuticals, volatile organic compounds and per- and polyfluoroalkyl substances at the USGS National Water Quality Laboratory (NWQL),...
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